CHAPTER 18  (cont.) - Lect.2

STANDARD STATES & STANDARD ENTHALPY CHANGES:

a) For a pure liquid or solid, the standard state IS the pure
    liquid or solid.
b) For a gas, the standard state IS the gas at 1 atm; in gas
     mixtures, its partial pressure must be 1 atm.
c) For solutions, the standard state is 1 M concentration.

  DHo means at standard pressure and T (STP) =
                        1 atm & 25oC (298K)

  DHfo is standard molar enthalpy of formation:  1 mole of a
    substance is formed from its elements in their standard
    states.  The DHfo for an element in its standard state = 0

    -DH = means giving OFF heat = EXOthermic
    +DH = means REQUIRING heat = ENDOthermic
 

Calculate how much heat is absorbed or evolved in the
        following reaction:

        2 NH3(g) + CO2(g) ----> NH2CONH2(aq) + H2O(l)

The DHo at 25oC (in kJ/mol):    NH3(g)  -45.9
                                                    CO2(g)  -393.5
                                                    NH2CONH2(aq)  -319.2
                                                    H2O(l)  -285.8

DHo = [319.2 - 285.8] - [2(-45.9) - 393.5] = -119.7 kJ.
    Because DHo is negative,  we conclude that heat is
    evolved and this reaction is exothermic.
 
 

Hess' Law of Heat Summation:
     Enthalpy change of a reaction is the same whether it
   occurs by one step or by many different steps.

Ex.:   C(s) + 2H2(g) ---> CH4(g)    DH= -4.28 kJ

C(s) + O2(g) ---> CO2(g)                         DH= -22.48 kJ
2H2(g) + O2(g) ---> 2H2O(l)                    DH= -32.66 kJ
CO2(g) + 2H2O(l) ---> CH4(g) + 2O2(g)   DH=+50.86kJ ________________________________

C(s) + O2(g) + 2H2(g) + O2(g) + CO2(g) + 2H2O(l) --->
                                   CO2(g) + 2H2O(l) + CH4(g) + 2O2(g)

Therefore, C(s) + 2H2(g) ---> CH4(g)
             DHo = -4.28 kJ/mol reaction

Therefore:DHo (reaction) = DHo (1) + DHo (2) + DHo (3) + ...
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Calculate DHo (reaction) for
            C2H4(g) + H2O(l) ---> C2H5OH(l)       from:

1)  C2H5OH(l) + 3O2(g) ---> 3H2O(l) + 2CO2(g)
                DH= -1367 kJ
2)  C2H4(g) + 3O2(g) ---> 2CO2(g) + 2H2O(l)
                DH= -1411 kJ

Take equation 2 as it is, and add to it equation 1
        (backwards)!! to get:

 C2H4(g) + + 3O2(g) + 3H2O(l) + 2CO2(g) --->
                     2CO2(g) + 2H2O(l) + C2H5OH(l) + 3O2(g)

Therefore:DHo (reaction) = DHo(2) - DHo(1) =
                                            = -44 kJ/mol reaction
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  DH°(reaction) = S nDH°(products) - S mDH°(reactants)

For CaO(s) + CO2(g) ---> CaCO3(s)

DH°(reaction) = S n[DCaCO3(s)] -
                                            S m[DCaO(s)+DCO2(g)]
DH°(reaction) = -1207 kJ - [-635.5kJ + (-393.5kJ)]
DH°(reaction) = -1207 kJ + 1029 kJ
                        = -178 kJ/mol reaction

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Calculate DH°(reaction) for:
                SiH4(g) + 2O2(g) ---> SiO2(g) + 2H2O(l)

D(reaction) = S [DH°SiO2(g) + 2DH°H2O(l)] -
                                          S [DH°SiH4(g)+2DH°O2(g)]
         = [-217.72 kJ + 2(-68.315 kJ)] - [+8.2 kJ + 2(0) kJ]
         = -217.72 - 136.63 - 8.2 = -362.6 kJ/mol reaction
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CalculateDHf°[PbO(s)] from:
                PbO(s) + CO(g) ---> Pb(s) + CO2(g)

Given:  DH°(reaction) = -65.69 kJ/mol reaction
             DHf°  CO(g) = -110.5 kJ/mol
             DHf°   CO= -393.5 kJ/mol
DH°(reaction) = S [DH° Pb(s) + DH° CO2(g)] -
                                            S [DH° PbO(s) + DH° CO(g)] =
     -65.69 kJ = [0 kJ + (-393.5 kJ)]
                                        - [DHf° PbO(s) + -110.5 kJ]
     -65.69 + 393.5 - 110.5 =  - DHf° PbO(s)
                   +217.3 kJ/mol =  - DHf° PbO(s)
                    -217.3 kJ/mol =  DHf° PbO(s)
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Calculate DHf°[NH3(g)] from:
                4NH3(g) + 7O2(g) ---> 4NO2(g) + 6H2O(l)

  Given:    DH°(reaction) = -1396 kJ/mol reaction
              DHf° NO2(g) = 34 kJ/mol
              DHf° H2O(l)  = -286 kJ/mol

   DH°(reaction) = S [4DH° NO2(g) + 6DH° H2O(l)] -
                                  S [4DH° NH3(g) + 7DH° O2(g)]
    -1396 kJ/mol = [4 (34 kJ) + 6(-286 kJ)] -
                                        [4DHf° NH3(g) + 7(0) kJ]
    -1396 kJ/mol = + 136 - 1716  - [4DHf° NH3(g)  + 0]
     +184 kJ/mol =  - 4DHf° NH3(g)
        -46 kJ/mol =  DHf° NH3(g)
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Bond Energies:  Amount of energy required to break 1
      mole of bonds in a gaseous covalent substance to
      form one mole of gaseous products at constant T & P.
                                H2(g) --- 2H(g)
 In order to break the H-H bond, we must supply
        436 kJ/mol.

 DH°(reaction) = DH° (H-H) = +436 kJ mol = endothermic
 

Therefore, we can get at the bond energies of simple
    molecules by measuring the heat required when bonds
    are ruptured.

Ex.:  CH4(g) + 2Cl2(g) + 2F2(g) --->
                                       CF2Cl2(g) + 2HF(g) + 2HCl(g)

CalculateDH°(reaction).
  Reactants ------------> Atoms -----------------> Products
              (energy required)        (energy released)

Reactant bonds broken:
 forCH4(g):  4 mol C-H = 4 mol (413 kJ/mol) = 1652 kJ
 for 2Cl2(g):  2 mol Cl-Cl = 2 mol (242 kJ/mol) = 484 kJ
 for 2F2(g):  2 mol F-F = 2 mol (155 kJ/mol)  =  310 kJ
                                               Total Energy required = 2446 kJ

Product bonds formed:
 for CF2Cl2(g): 2 mol C-F = 2 mol (485 kJ/mol) = 970 kJ
                        2 mol C-Cl = 2 mol (339 kJ/mol) = 678 kJ
 for HF(g): 2 mol H-F = 2 mol (565 kJ/mol) = 1130 kJ
 for HCl(g): 2 mol H-Cl = 2 mol (432 kJ/mol) = 864 kJ
                                               Total Energy released = 3642 kJ

DH°(reaction) = Energyrequired to break bonds -
                                        Energy released in forming bonds
       = 2446 kJ - 3642 kJ = -1196 kJ/mol CF2Cl2(g) formed
     Therefore, since Dis - , this reaction is EXOthermic.
 

Changes in Internal Energy DE:

DE = E(final) - E(initial) = q + w ,
                    where q = heat and w = work

       work = fd  (force x distance)

DE = (am't of heat absorbed by system) +
                                (am't of work done on the system)

 When q = + : heat is absorbed by system from the
                                surroundings
 When q = -  : heat is released by system to the
                                surroundings
 When w = + : work is done on the system by the
                                surroundings
 When w = -  : work is done by system on the
                                surroundings
 
 

The ONLY TYPE OF WORK  in physical & chemical changes
                is PRESSURE-VOLUME work.

 w = - PDV       DE = E(final) - E(initial) = q + w   = q - PDV

  1)  compression of gas:  work done BY surroundings ON
        the system (to compress a gas, you must SUPPLY
        energy)
        w = -P(Vf-Vi):  since Vf is smaller than Vi , w = +

     *decrease in the number of moles of gas;
                    therefore:  Dn = -1
         Ex.:  2H2(g) + O2(g) ---> 2H2O(g);  Dn = 2 - 3 = -1

  2)  expansion of gas:  Work done BY the system ON the
        surroundings (if you let a gas expand, you will get
        energy released)
        w = -P(Vf-Vi):  since Vi is smaller than Vf , w = -
 
   *increase in the number of moles of gas;
                    therefore:  Dn = +1
         Ex.:  2H2O(g) ----> 2H2(g) + O2(g);   Dn = 3 - 2 = 1
 

When the VOLUME is constant, NO PDV work done.
            Therefore, DE = qv

When the PRESSURE is constant, -PDV = -DnRT =
                work done.
   Therefore, the only time there is work done is when Dn is
   NOT zero; i.e., when there is a change in the number of
   moles of gaseous products and reactants, so that the
   volume of the system changes.
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Bomb Calorimeter:  A closed volume system where a
    sample is burned, usually in the presence of oxygen.
    Of course, the pressure increases, but so also does the T.

 The heat liberated here is
                 qv = DE (constant volume) = INTERNAL ENERGY

Ex.:   C6H6(l) + 15/2[O2(g)] ----> 6CO2(g) + 3H2O(l)

When 0.187 g of benzene, C6H6, is burned in a bomb
    calorimeter, the surrounding water bath rises in
    temperature by 7.48oC.  Assuming that the bath contains
    250.0 g of water and that the calorimeter itself absorbs
    2.56 kJ, calculate the combustion enthalpy for benzene
    in kJ/mol.

The amount of heat responsible for the increase in T of the
        water is:
  heat required = (7.48oC)(4.184 J/g-oC)(250.0 g) = 7824 J
The amount of heat responsible for the heating the
        calorimeter = 2.56 kJ = 2560 J

Total amount of heat absorbed by calorimeter and water =
                    10384 J

Therefore, the combustion of 0.187 g of benzene liberates
                    10.384 kJ of energy.

     DE (internal energy) = -10.384 kJ/0.187 g benzene
    Therefore, DE = (-10.384 kJ/0.187 g benzene)X
                                            (78.0g benzene/mol) =
      DE  = -4331 kJ/mol benzene   OR /mol reaction.
           Remember:  Constant V !!!!
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Relationship between DH and DE:
 

DH = DE + PDV  (at constant T & P)

But we know that DE = q + w

   Therefore, DH = q + w + PDV  (at constant T & P)

At constant P, w = -PDV

    Therefore, DH = q -PDV + PDV = qp
 

The difference between DE and DH is the amount of
    expansion
work (PDV work):  DH = DE + (Dn)RT 
        (at constant T & P)

Ex.:  CH4(g) + 2O2(g) -----> CO2(g) + 2H2O(g)

 DHo (at 25oC and 1 atm)= -890 kJ.  Calculate DE.
            Since  Dn = (2-2) = 0,
    there is NO PDV work;  DE = DHo = -890 kJ
 

Ex.: N2(g) + 3H2(g) -----> 2NH3(g); DH = -91.8 kJ.
       Calculate DE at 25oC.
           DH = DE + DnRT; DE = DH - (Dn)RT
             = -91.8 kJ -[(2-4 moles)(8.314J/mol-K)(298K)
             = -91.8 kJ + 4955 J = -91.8 kJ + 5.0 kJ
             = -86.8 kJ/mol reaction
 

Ex.:  C2H5OH(l) + 3O2(g) ----> 2CO2(g) + 3H2O(l)
      Dn = 2 - 3 = -1    REMEMBER!!!   ONLY MOLES OF GAS!!!
 

BOTTOM LINE: DH = qp at constant P (usually
                                                            atmospheric P)

   DE = qv at constant V (bomb calorimeter experiment)
    DH = DE when there is NO WORK done; no PDV, no (Dn)RT
      DH = DE + (Dn)RT when there IS work done
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Spontaneous Processes:
Occur without outside intervention, e.g., drop two eggs...
        they break!
   The reverse process is non-spontaneous.
The direction of a spontaneous process can depend on
        temperature.
     Ice turning to water is spontaneous at T > 0°C.
     Water turning to ice is spontaneous at T < 0°C.
Allowing 1 mol of ice to warm up is an irreversible process.
To get the reverse process to occur, the water temperature
        must be lowered to 0°C (heat must be removed).
In any spontaneous process, the path between reactants
    and products is irreversible, unless outside intervention
    occurs.
E.g., water can be frozen...then thawed by adding heat.
Thermodynamics gives us the direction of a process, but
    not the speed at which it will occur (this latter is
    KINETICS).

    Why are endothermic reactions spontaneous?
 

Entropy and the Second Law of Thermodynamics:
Consider an initial state: two flasks connected by a closed
    stopcock.  One flask is evacuated and the other contains
    1 atm. of a gas.  Then open the stopcock....The final
    state: two flasks connected by an open stopcock.

    Each flask contains the gas at 0.5 atm.  The expansion
    of the gas is isothermal (i.e., constant temperature).
    Therefore, the gas does NO work and heat is not
    transferred.

    Why does a gas expand?

ENTROPY!  S:  is a measure of the disorder of a system.
    The bigger the disorder.....bigger entropy.
            More order.....lower entropy (ice is more ordered
            than water, which is more ordered than steam).

 Spontaneous reactions proceed to lower energy or
              higher entropy.

    In the connected flasks, is it more likely that all the gas
    molecules stay in one flask or that they spread out
    randomly to fill both flasks?  The molecules are more
    likely to fill both flasks, and the system has moved to a
    state of higher entropy.

What about thawing ice?
    In ice, the molecules are very well ordered because of
    the H-bonds throughout the system (and the molecules
    of water are in fixed positions); therefore, ice has a low
    entropy.  As ice melts, the intermolecular forces are
    broken (which requires energy), but the order is
    interrupted, so entropy increases.  Water is more random
    than ice, so ice spontaneously melts at room
    temperature.  There is always a balance between energy
    and entropy considerations.
 

    Generally, an increase in entropy in one process is
    associated with a decrease in entropy in another; the
    increase in entropy usually dominates.
 

Entropy is a state function.

For a system, DS = Sfinal - Sinitial
If DS > 0, the randomness increases (less order);
            if  DS < 0, the order increases.

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