CHAPTER 14 CHEMICAL KINETICS - LECTURE 1:

Many reactions which are thermodynamically feasible are
    not kinetically feasible.

O2(g) + H2(g) -----> H2O(g) DH = -241.8 lK/mol reaction
tells us that the reaction is allowed to go
thermodynamically.

However, if we try the experiment, we will wait for a
VERY
long time, because the KINETICS for this reaction
are extremely slow.

14.1 Rate of reaction = speed of reaction = positive
    quantity that tells us how [reactant] or [product]
    changes with time.

Or: how quickly products are made or reactants are
      used up.

Consider:  aA + bB ----> cC + dD, where the lower case
    letters are the coefficients in the balanced equation
    and the upper case are the chemical species.

 Rate of reaction = -(D[A])/aDt = -(D[B])/bDt
                loss of A or loss of B with time
                             = (D[C])/cDt  = (D[D])/dDt
                gain of C or gain of D with time

    Ex.:  H2(g) + 2ICl(g) -------> I2(g) + 2HCl(g)

    Rate of reaction = -(D[H2])/Dt = -(D[ICl])/2Dt
                                =  (D[I2])/Dt = (D[HCl])/2Dt


Data:

 [H2]              [ICl]        time(sec)     rate = -(D[H2])/Dt
                                                                    = -(D[ICl])/2Dt  
 0.750            1.500            0

 0.424            0.848            1            > 0.326 Ms-1
 0.276            0.552            2            > 0.148
 0.186            0.372            3            > 0.090
 0.124            0.248            4            > 0.062
 0.078            0.156            5            > 0.046

    Plot [] as a function of time.
 

Instantaneous rate of reaction at any time t is -slope of
    the
tangent to the curve at that time t.

Rate at time 4 sec.  =  -slope of the tangent at 4 sec.
        rate = (-slope) = -(rise/run) = -Dy/Dx
                                  = -[(.06-.35)/(5-0)]
                                  = -(-0.29/5) = 0.058 Ms-1
 

At t = 0, instantaneous rate = -Dy/Dx
                                              = -(0.600-0.750)/(0.5-0.0)
               (from [H2])            = -(-0.300) = 0.300 Ms-1

OR: instantaneous rate=-Dy/2Dx=-(1.20-1.50)/(0.5-0.0)
               (from [ICl])   = -(1/2)(-0.30/-0.5)=0.300 Ms-1

NOTE:  get the same instantaneous rate from either
            reactant!!
- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -

Average rate over some time:
    EX: average rate over the 1st 3 sec.:

    average rate = -(D[H2])/Dt = -(0.186-0.750)/(3-0)
                          = -(-0.564/3) =  0.188 Ms-1


    EX: average rate for the 1st 5 sec.:

    average rate = -(D[H2])/Dt = -(0.078-0.750)/(5-0)
                          = -(-0.672/5) =  0.134 Ms-1

 

Ex.:  Iodide ion is oxidized by hypochlorite ion in basic
         solution:

                I-1(aq) + ClO-1(aq) ---> Cl-1(aq) + IO-1(aq)

In 1.00 M NaOH at 25oC, the [I-1] at different times was
    measured to be:
                 time:  2.00 s            8.00
                 [I-1]:  0.00169        0.00101

Calculate the average rate of the oxidation of I-1 during
        this time interval.
      average rate = -[DI-1]/DT
                             = -[(0.00101-0.00169)/(8.00-2.00)]
                             = 1.13 X 10-4 Ms-1
- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -

Rates of chemical reactions are affected by:

    1)  concentrations of reactants:  usually the higher the
          concentrations, the faster the reaction.
    2)  T of the reaction:  usually the higher the T, the faster
          the reaction.  Therefore, bacterial spoilage of food is
          slowed by lowering the T (refrigerator).
    3)  catalyst:  the rate of a reaction is usually increased
          by adding a catalyst, without the catalyst being used
          up.
    4)  surface area of solid or liquid reactants or catalysts:
          the larger the surface area, the faster the reaction.


     Ex.:  2 N
2O5(g) ----> 4 NO2(g)   +  O2(g)

        rate of formation of O2 = 1/4 rate of formation of NO2
                                      = 1/2 rate of decomposition of N2O5
 

14.2 The Rate Laws
    Dependence of the Rate on Concentration:
            called the    rate law

                rate = k[A]x[B]y[C]z

the coefficients x, y, z can ONLY be found by experiment !!!

Experimental Determination of Rate Laws:
    We will study the rate of a reaction by measuring the
    instantaneous rate at t = 0 for each reactant in the
    equation (initial rate of reaction).

    Ex.:    2 NO(g) + Cl2(g) ----> 2 NOCl(g)

                          [NO]    [Cl2]     initial rate (Ms-1)
          exp.1      0.10      0.10    2.53 x 10-6
          exp.2      0.10      0.20    5.06 x 10-6
          exp.3      0.20      0.10    10.1 x 10-6
          exp.4      0.30      0.10    22.6 x 10-6

                rate = k[NO]x[Cl2]y

1)  compare exps. 1 & 2:
  rate 2 = 5.06 x 10-6   = k[NO]x[Cl2]y= k(0.10)x(0.20)Y
  rate 1     2.53 x 10-6        k[NO]x[Cl2]y     k(0.10)x(0.10)Y

   5.06 x 10-6  = 2 = (0.20/0.10)y = 2y    Therefore,  y = 1
  2.53 x 10-6
 

2)  compare exps. 1 & 3:
  rate 3 = 10.1 x 10-6  = k[NO]x[Cl2]y= k(0.20)x(0.10)Y
  rate 1     2.53 x 10-6     k[NO]x[Cl2]y      k(0.10)x(0.10)Y

  10.1 x 10-6 = 4 = (0.20/0.10)x = 2x     Therefore,  x = 2
 2.53 x 10-6

            Therefore, rate = k[NO]2[Cl2]1

 2nd order with respect to NO and 1st order with respect
        to Cl2 , and 3rd order overall.

  Find k, the reaction rate constant:
        Using data from Exp. 1:
         2.53 x 10-6 Ms-1= k(0.10 M)2(0.10M)1
             2.53 x 10-6Ms-1/(0.10 M)2(0.10M)1 = k
             2.53 x 10-3M-2s-1 = k

OR:  Using data from Exp. 4:
         22.6 x 10-6 Ms-1= k(0.30 M)2 (0.10M)1
              22.6 x 10-6Ms-1/(0.30 M)2 (0.10M)1 = k
              2.51 x 10-3M-2s-1 = k

                    THEREFORE, k = constant!!!

BACK HOME